ɫVһNxØƷиMc(dng)̶ͬ(QϵIJ)Ȍxһzy(c)Mּ京ķ
2 ɫVķxԭ
(dng)S(dng)(jng)ɫVr(sh)͕(hu)cй̶l(f)(ܽ)ڻиMW(xu)|(zh)ͽY(ji)(gu)ϵIJc̶l(f)õĴС(qing)ͬͬһƄ(dng)Mڹ̶еĜr(sh)gͬĶʹиMְһ@NøMڃϵIJʹиMַxļg(sh)QɫV
3 (dng)ࣺɫVx^ДyMǰƄ(dng)|(zh)
4 ̶ɫVx^вƄ(dng)ľԵĹwͿndwҺw
5 ɫVc(din)
(1)xЧʸ(f)sЙC(j)ͬϵ(gu)w(2)`ȸԙzy(c)μg.g-1(10-6)(j)ng.g-1(10-9)(j)|(zh)(3)ٶȿһڎ犻ʮ犃(ni)һ(g)ԇӵķ(4)(yng)÷VɫVc(din)400ĸNЙC(j)oC(j)ԇӵķҺɫV߷c(din)(wn)ԇӵķx(5)x:(du)|(zh)OƵĽMк(qing)ķx֮̎xMֵĶ^y
6 ɫVķB(ti)ʽxԭ
7 B(ti)
ɫV(Gas Chromatography, GC)ҺɫV(Liquid Chromatography, LC)RwɫV (Supercritical Fluid Chromatography, SFC)ɫV(dng)w(Qd)õĚɫV(dng)N2H2HeȚwxͬɷ֞飺ɫVë(x)ɫV;̶IJַͬ֞飺ɫV͚ҺɫVҺɫV(dng)Һw(ҲQϴҺ)̶IJͬ֞飺ҺɫVҺҺɫVRwɫV(dng)鳬RwRwһNښwҺw֮gĠB(ti)RwɫVǼɫVҺɫVă(yu)(sh)l(f)չһN͵ɫVxg(sh)H܉ɫV˷ĸ߷c(din)͓]l(f)ԵԇӽM֣ҾбȸЧҺɫVķʺߵЧ
8 ʽ
ɫV(Column Chromatography, CC):̶b܃(ni);ɫVë(x)ɫVɫV(Paper Chromatography, PC)̶V;m(dng)܄ʹƷڞVչ_M(jn)зxɫV(Thin Layer Chromatography, TLC)
̶ɻͿɱ;ͬɫV
9 xԭ
ɫV(Absorption chromatography);ɫV(Partition Chromatography);xӽQɫV(Ion Exchange Chromatography);zɫV(Gel Chromatography)
10 ɫVD
Mڙzy(c)Ϯa(chn)̖(ho)(qing)Ȍ(du)r(sh)g(t)ĈDӛ˸MɫVrֽɫVͻַQɫV
11 ɫVֵ
ɫVֵɫVԷ(j)wF(xin)˸y(c)MɫVϵĜrڹ̶ܽԽc̶Խ(qing)ĽMеĜr(sh)gԽL(zhng)fM֎ɫV(dng)weԽԱֵñr(sh)gͱweׅ(sh)
12 ɫVDϵɫVfʲô}
(j)ɫVĔ(sh)ĿДƷMֵق(g)(sh);(j)ɫVıֵM(jn)жԷ;(j)ɫVeM(jn)ж;(j)ɫVıֵͅ^(q)?q)u(png)r(ji)ɫVķxЧ;(j)ɷgľxu(png)r(ji)̶༰(dng)xǷm
13 ָһضMڃg_(d)ƽr(sh)|(zh)
14 ɫVɷ֮gľxҪɃɽMڃgķϵ(sh)߀ǔU(ku)ɢٶțQ?ʲô?
𣺷ϵ(sh)ɷgľxɟW(xu)؛QɽMڃзϵ(sh)ԽɷgľxtԽԽױxU(ku)ɢٶDŽ(dng)W(xu)ӳɫVϼɫVą^(q)?q)?Π)
15 ɫVՓҪQĆ}
ɫVx^̵ğW(xu)̈́(dng)W(xu)}Ӱ푷xЧcЧ;Чcxȵu(png)r(ji)ָ(bio)P(gun)ϵ
16 Mֱr(sh)gβͬ?ɫV׃?
Mֱr(sh)gɫV^̵ğW(xu)ؿ;(M̶ֺҺĽY(ji)(gu)|(zh))ɫV׃ɫV^̵Ą(dng)W(xu)ؿ;(е\(yn)(dng)U(ku)ɢ)ՓՓքeğW(xu)̈́(dng)W(xu)ĽǶUɫVxЧܼӰ
17 뽛(jng)(yn)Փ
ɫVx^̱ȔMs^Bm(x)ɫVx^̷ָɶεƽ^̵؏(f)(sϵƽ^)
18 Փc(din)
Փ唵(sh)߶Чĺָ(bio);ͬ|(zh)ͬһɫVϵķϵ(sh)ͬЧ唵(sh)Ч߶Чָܵ(bio)r(sh)(yng)ָy(c)|(zh);ЧܱʾxMֵČ(sh)HxЧ(dng)ɽMֵķϵ(sh)Kͬr(sh)oՓԓɫV唵(sh)ox
19 ՓIJ㣺
ՓĻO(sh)ɫVČ(sh)Hx^̡ՓoͬһɫVڲͬ(dng)ЧͬČ(sh)(yn)Y(ji)fɫVʲô(hu)չͬr(sh)δָӰЧؼЧ;ͷ
20 ʷ̣
(ҲQķطʽ)H = A + B/u + C·u H߶; u(dng)ƽٶ(cm/s)
A uU(ku)ɢ(xing) Ac(dng)|(zh)(dng)ʟoP(gun)ҪpСAֵҪ߹̶w(x)Ⱥ;ԼԁQ(du)ڿë(x)A=0̶wԽСdp↓ԽA↓H↓Чn↑F(xin)ڜuU(ku)ɢɫV׃F(xin)ppɫV^խ
B/u —ӔU(ku)ɢ(xing) Ȳa(chn)vU(ku)ɢ;U(ku)ɢ(do)ɫV׃H↑(n↓)x׃;;ӔU(ku)ɢ(xing)cP(gun)↓r(sh)g↑U(ku)ɢ↑;U(ku)ɢϵ(sh)Dg ∝(Md)-1/2 ; Md↑Bֵ↓
C ·u —|(zh)(xing) dp↓ df↓, D ↑ ,ɽ͂|(zh)
21 H - u c٣
ٌ(du)@(xing)ȫ෴ãٌ(du)ЧĿӰʹôһ(g)ֵʷʽ߶Ȍ(du)ٵһA(do)(sh)һOСֵ߶H(du)(yng)uDc(din)ټ١
22 ՓҪc(din)
Mַ(ni)\(yn)еĶ·cuU(ku)ɢݶɵķӔU(ku)ɢ|(zh)ʹgķƽⲻ˲g_(d)ɫVU(ku)չЧ½Ҫԭ;ͨ^xm(dng)?sh)Ĺ̶dNҺĤȼdٿЧ;ՓɫVxͲlxṩՓָ(do)Uٺ،(du)ЧxӰ;NƼsdӔU(ku)ɢ(xing)Ӱ표pСʹЧͬr(sh)|(zh)(xing)ӰʹЧ½;ڂ|(zh)ּӄ˷ӔU(ku)ɢӰxїlʹЧ_(d)
23 ɫVԷ
1 c(bio)ӌ(du)յķ ñֵԣͨ^(du)ԇоc|(zh)ֵͬɫV壬_ԇǷԓ|(zh)ɫVDеλmڲͬxϫ@õĔ(sh)(j)֮gČ(du)ü뷨ԣ|(zh)뵽ԇ^MɫV(du)׃2 īI(xin)ֵ (du)ֵr21(du)ֵr21Hcغ̶|(zh)P(gun)ɫVփ(c)жиN|(zh)ڲ̶ͬϵı(sh)(j)ÁM(jn)жb
24 ɫV
1 УӣԇиM|(zh)cɫVem i = fi’ ·Ai ;^(du)Уӣϵ(sh)f i λe(du)(yng)|(zh)f i ’ =m i / Ai ;(du)Уf i MֵĽ^(du)Уc(bio)(zhn)|(zh)Ľ^(du)У֮ȡ
2 õĎN
1wһc(din)Ҫwһ(jin)㡢(zhn)_;M(jn)Ĝ(zhn)_ԺͲl׃(dng)(du)y(c)Y(ji)Ӱ푲;HmԇнMȫr
2(bio) ——(bio)(zhn)c(din)Ҫ(bio)ʹУ(zhn)_^l׃(du)Y(ji)(zhn)_Ӱ^(du)M(jn)Ĝ(zhn)_ԿҪ^mڴԇӵĿٷ
3(ni)(bio)(ni)(bio)ҪMҪ(a)ԇвԓ|(zh);(b)cy(c)M|(zh)^ӽ;(c)cԇӰl(f)W(xu)(yng);(d)λÑ(yng)λڱy(c)Mָܷx_;(e)mвcy(c)Mֽӽ(ni)(bio)c(din) (ni)(bio)Ĝ(zhn)_^lM(jn)S׃(dng)(du)Y(ji)Ӱ푲;ÿ(g)ԇӵķҪM(jn)ЃɴηQmϴԇӵĿٷ;(ni)(bio)еԇȡ̓(ni)(bio)̶twi=Ai/As *(sh)
ɫV
1 ɫV(GC )Ԛw(dng)ɫV
2 ɫVҪƷ⻯ mڴַc(din)ߺ͟(wn)Ļ(du)ڸgܺͷ(yng)^(qing)|(zh)yڷ
s15%-20%ЙC(j)ÚɫVM(jn)з
3 ɫVxĽMɣ·ϵy(tng)M(jn)ϵy(tng)xϵy(tng)zy(c)ϵy(tng)ؿϵy(tng)ӛϵy(tng)
4 ·ϵy(tng)Դdٿ;õdУ?d)?/span>
5 M(jn)ϵy(tng)M(jn)bú͚⻯ҡwM(jn)(ͨy)ԇȳMdyеԇӚwM(jn)x;ҺwM(jn)ͬҎ(gu)עɫV10μL;ë(x)ɫV1μL;̓xȫԄ(dng)ҺwM(jn)ϴ(rn)_ȡӡM(jn)Qӵ^Ԅ(dng)ɣһοɷÔ(sh)ʮ(g)ԇ
6 M(jn)ӷʽM(jn)ӣƷ҃(ni)⻯ֽ(jng)ܵſֻИOСһֱd⌧(do)ɫV;M(jn)ӣƷֱעɫVң(jng)^]l(f)ȫɫV
7 xϵy(tng)ɫV(2-6 mmֱ1-5 mL(zhng))ë(x)(0.1-0.5 mmֱ, ʮL(zhng))
8 ؿϵy(tng)ãضɫVxlҪx(sh);:⻯ɫVzy(c)ɫVxr(sh)Ɯض;⻯ңCҺwԇ˲g⻯;zy(c)CxĽMͨ^r(sh)ڴ;ɫV䣺(zhn)_ƷxҪĜضȡ
9 zy(c)ϵy(tng)ãɫVxĸMֵD(zhun)׃ɿɜy(c)̖(ho)ָ(bio)`Է푑(yng)ٶȡY(ji)(gu)ͨͨ——(du)|(zh)푑(yng);
——(du)ض|(zh)и`푑(yng)zy(c)͙ͣzy(c)ጧ(do)zy(c)Ӳ@zy(c);|(zh)͙zy(c)xӻzy(c)șzy(c)
10 ጧ(do)zy(c)Ҫc(din)Y(ji)(gu)(jin)(wn)Ժ;(du)oC(j)ЙC(j)ﶼ푑(yng)ƉĘƷ;`Ȳ
11 xӻzy(c)c(din)(yu)c(din)(1)͵|(zh)͙zy(c);(2)͙ͨzy(c)(y(c)CЙC(j));(3)zy(c)нY(ji)(gu)(jin)(wn)Ժá`ȸ푑(yng)ѸweСԷc(din);(4)ȟጧ(do)zy(c)`ȸ߳3(g)(sh)(j)zy(c)_(d)10-12g·g-1ȱc(din)(1)(du)dҪ(2)zy(c)r(sh)ҪƉĘƷoƷ(3)ܙzy(c)ԚwˮȻ̼
12 ӷ@zy(c)c(din)(du)uк(qing)푑(yng);`ȸߣںr(nng)ˎķ;Է^խ
13 șzy(c)(FPD)һN(du)иxԵęzy(c)ڸȼЙC(j)Ƭl(f)ͬL(zhng)V
14 ̶ࣺw̶ࣺw;Һw̶ࣺdw̶ҺM;ۺ̶
15 w̶ࣺһwõл̿zXͷӺY(yu)c(din)᷀(wn)Ժr(ji);ȱc(din)ЧжʹǰҪM(jn)л(yng)ãҪڶԚwH2O2N2COCO2CH4һw͵ͷc(din)|(zh)
16 dwʹõ|(zh)(yng)MėlY(ji)(gu)ȱe;W(xu)ԣcƷMֲW(xu)(yng)oû;᷀(wn)Ժ;һęC(j)е(qing)Ⱥͽ(rn);һȺҎ(gu)tΠ
17 (du)̶ҺҪʹÜضҺw^͵ē]l(f);õğ᷀(wn);(du)ҪxĸM֑(yng)кmķϵ(sh);W(xu)(wn)ԺcƷMddwl(f)κλW(xu)(yng)
18 ̶ҺķǘOԹ̶ҺеȘOԹ̶Һ(qing)OԹ̶ҺI̶Һ
19 ǘOԹ̶ҺҪһЩNͼͣcy(c)|(zh)֮gɫɢMְc(din)ɵ͵ƷмИOԺͷǘOԽMtͬc(din)ĘOԽMȳõĹ̶Һн?f)?ʮ)ƤɵȡmڷǘOԺOԻķ
20 еȘOԹ̶Һ^ĘOԻF(tun)T(do)OĻF(tun)Mcy(c)|(zh)gɫɢT(do)Mֻϰc(din)ͬc(din)ķǘOԽMȳõĹ̶ҺȣmOԺеȘOԻķ
21 (qing)OԹ̶Һ^(qing)ĘOԻF(tun)cy(c)|(zh)goT(do)MְOСõĹ̶ҺmژOԻķ
22 I̶ҺǏ(qing)OԹ̶Һһcy(c)|(zh)gԚIMγɚIy׳̶ȳγɚIĽMȳõĹ̶ҺоҶҴmڷF(xin)NOȵĻ
23 ̶ҺxٰOԭtxOܽȴϵ(sh)r(sh)gL(zhng):ڰ܈F(tun)x---̶Һ;---Ҷ̶Һ۰ҪexMgc(din)Ҫe----ǘOԹ̶Һ;OԞҪe----OԹ̶ҺxϹ̶Һ(du)yxď(f)sƷxÃɷNɷNϹ̶Һ
24 ۺ̶ࣺȿw̶࣬ҲdwַQ߷Ӷ|(zh)ȴִܽ(1)^ıȱe(2)(du)ǘOԼO|(zh)oкβF(xin)СOԽMҲܳ(du)Q(3)ڲҺĤoʧF(xin)᷀(wn)Ժ(4)C(j)е(qing)Ⱥg^ϵΣɫVоԡجF(xin)ԺڜpٜuU(ku)ɢ
25 dNxzy(c)m(yng);dٵĴС
26 صx
(1)ȑ(yng)ʹؿڹ̶ҺʹÜض(^ԓضȹ̶Һʧ)ʹÜض(ڴ˜ضȹ̶ҺԹwʽ)֮(ni)
(2)أԸƂ|(zh)Чs̷r(sh)gӺxڷxһԭtǣʹyxĽMֱMܷxǰ£M^͵Աr(sh)gmββȡ
(3)һxڽӽԵڽMƽc(din)r(sh)Ĝض
(4)M֏(f)sг̌ԇóء
27 dw̶Һxȣ̶ҺdwϵͿnһָǹ̶Һc(dn)wİٷֱͨ5%25%֮gԽ(dn)wγɵҺĤԽ|(zh)ԽСЧԽٶҲԽ^͕r(sh)̶ؓ(f)dSM(jn)^СͨAʹ^͵
28 M(jn)ӗlxM(jn)(yng)Szy(c)ԙzy(c)֮(ni)M(jn)Ҫ(dng)r(sh)g;⻯һ^ظ30~70°C
29 ɫVx;(1)ՓL(zhng)pС唵(sh);(2)ՓpСMеĜuU(ku)ɢ͂|(zh)ɽ߶
30 ë(x)ɫVĽY(ji)(gu)c(din)
(1) bСL(zhng)ȿ_(d)ë(x)0.2mm
(2);ͨ^˽MеĜuU(ku)ɢ
(3)̶ҺֱͿڹܱ(ni)e^,ͿӺܱtҺ|(zh)͡
(4)ë(x)ɫVЧ_(d)ÿ30004000KՓһ֧L(zhng)100ë(x)Փ唵(sh)_(d)104106
31ë(x)ɫV(yu)c(din)
(1)xЧʸߣ10100
(2)ٶȿ죺ë(x)ɫVɫVٶ
(3)ɫVխΌ(du)Q^óطʽ
(4)`ȸһÚzy(c)
(5)uU(ku)ɢ㡣
32ë(x)ɫVͣ
(1)Ϳë(x)̶ҺֱͿڹ܃(ni)(du)(jin)ƂجF(xin)Բ̡
(2)ë(x)ڹܱͿһӶw(gu)ë(x)ܚɫV
(3)dwͿnë(x)dz(x)ē(dn)wճڹܱϣͿ̶ҺЧ^Ϳë(x)
(4)W(xu)Iϻ(lin)ë(x)̶Һͨ^W(xu)(yng)Iڹܱϻ(lin)һʹЧM(jn)һ
ЧҺɫV
1 cɫVҺɫVă(yu)c(din)cɫVҺɫVܘƷ]l(f)Ժ᷀͟(wn)Լ(du)|(zh)ֻҪјƷƳҺdzmڷxxͻ(wn)Ȼa(chn)ԼN߷ӻҺɫV(dng)HʹƷɫVƄ(dng)c̶һcƷӰl(f)xԵ@͞ƺƷxlṩһ(g)~Ŀ׃ءɫVõ(dng)ǶԚw(du)M֛]HH\(yn)d
2 ҺɫVc(din)߉Ч`߷c(din)(wn)ЙC(j)ԇӵĸЧx
3 ЧҺɫVxĽMɣ߉ݔҺϵy(tng)M(jn)ϵy(tng)xϵy(tng)zy(c)ϵy(tng)(sh)(j)̎ϵy(tng)
4 (dng)ʹǰÓ⣺õÓⷽ ͉Óⷨ(늴Ŕˮóͬr(sh)ӟ܄?d)?ÓⷨͳÓⷨ
5 ݶϴÓÃɷN(N)ͬOԵ܄ڷx^аһBm(x)׃(dng)܄Ⱥ͘Oͨ^(dng)ИOԵ׃׃xMֵķx߷xЧ
6 ߉ݶ((ni)ݶ)c(din)ȼӉ܄ø߉ԺݔɫVϵy(tng)ݶȻԻϺɫV
͉ݶ(ݶ) c(din)ȻϺӉڳA(y)Ȱһij?q)܄ϺñݔɫV
7 M(jn)ϵy(tng) ҪõܷԣСweõķ(wn)M(jn)ӕr(sh)(du)ɫVϵy(tng)Ӱ^С
8 xϵy(tng)ɫVnj(sh)F(xin)xĺIJ̶ܺMܞֱͲP䓹ܡһɫVL(zhng)5~30 cm(ni)4~5 mmzɫV(ni)3~12 mmƂɫV(ni)t_(d)25 mmһϴ܄M(jn)ɫVx֮ǰͨ^ǰHPLCwһs3~10 m䳣Ä{ɫVİl(f)չڅ(sh)ǜpСȺЧ
9 zy(c)ϵy(tng)——ÁBm(x)O(jin)y(c)(jng)ɫVxĽMɺͺ׃b-Ҋՙzy(c)늶OЙzy(c)ʾ۹zy(c)ɹzy(c)늻W(xu)zy(c)
10 ЧҺɫV(du)(dng)Ҫ(dng)cɫVl(f)滯W(xu)׃ԱЧӵı|(zh)^L(zhng)r(sh)g׃;(du)y(c)Ʒܽ;cÙzy(c)ƥ;ճȱMСԫ@^ߵЧ;(dng)༃Ҫr(ji)С
11 ЧҺɫVĹ̶ķ
(1)̶܉֣ԹwԶ|(zh)ɳ^߉IϸNܹ܈F(tun)---IϹ̶Ŀǰ(yng)VĹ̶ӲzҪxӽQɫVzɫVɾ۱ϩcϩ(lin)ɳܵĉ^͡
(2)϶ȷ֣ͣwβڲͿһӶ|(zh)zXxӽQ֬ӺYȡ(yu)c(din)mڿٷxoܡC(j)е(qing)ȸܸܳ߉mں(jin)εĘƷҎ(gu):ȱc(din)ӱM(jn)ȫͣɹzwۼɣȱeСwȫ̶\|(zh)ʿЧxЧmڏ(f)sƷMֵķxĿǰHPLCБ(yng)VĹ̶
12 ҺɫVԭԹw̶Ļľԇӷӱ(dng)(ni)r(sh)c(dng)܄l(f)(jng)(zhng)x^һ(g)-ƽ^
13 ҺɫV̶ࣺͨǹzX̿ȹwz(dng)ࣺOԴԇØOԏ(qing)ϴÓOԇØOϴÓ(yng) ή(gu)wxxr(nng)ˎ(gu)w;ʯ顢ϩNķxmڏ(qing)OԵx͘Ʒķxmڷxͬϵ(?yn)?du)(du)|(zh)x^С)
14 ҺҺɫVԭ(j)|(zh)ڃɷN(ֻ)ҺwܽȵIJͬ(sh)F(xin)xϵ(sh)^ĽMֱֵҲ^
15 ҺҺɫV(dng)ࣺ(dng)c̶Һ(yng)M߶ߵĘOԽԽ(j)(dng)c̶OԵIJe̶ɌҺҺɫV֞ɫV((dng)OСڹ̶OOСmڏ(qing)OԺеȘOԽMַx)ͷɫV((dng)OԴڹ̶OOԴmڷǘOԻOԽMַx)̶ dw̶ҺMõĹ̶Һb,b’-Ҷʮ?f)ȡ?yng) ͬϵMֵķxxˮ⵰|(zh)ɵĸNx֬ͬϵ
16 W(xu)IϹ̶ࣺW(xu)IϹ̶ûW(xu)(yng)ЙC(j)Iϵdwγɾһι̵ĆηӱӶ(gu)ɸNܵĹ̶
17 W(xu)IϹ̶c(din)̶ʧķ(wn)Ժ͉^;ܸN܄ݶϴÓ;^һ]Һ|(zh)Ч;IϲͬF(tun)Ը׃xԡIȘOԼF(tun)ɫVIxӽQF(tun)xɫVIC2C4C6C8C18C16C18C22ͱȷǘOԻF(tun)ڷɫVHPLC^Ĺ̶
18 xӽQɫVԭxӽQɫVĹ̶xӽQ֬(dng)ˮҺôy(c)ƷиMxcxӽQ֬HIJͬM(jn)зx
19 xӽQɫV(dng)ࣺˮľ_ҺxxӽQ̶֬ˮҺ;xxӽQ̶֬࣬ÉAˮҺ;(yng)ãxӼxĻ
20 zɫVԭzɫVĹ̶z|(zh)(dng)ˮҺЙC(j)܄Ǹ(j)ͬMַweĴСM(jn)зxġСӿԔU(ku)ɢz϶ͨ^;еȷֻͨ^z϶ͨ^;ӱų;܄Сȫweǰ;Ɍ(du)(du)|(zh)100-105(ni)Ļﰴ|(zh)x
21 zɫV(dng)ࣺܽƷcz((rn)zֹ)ճС(ӔU(ku)ɢٶ)Ěȷ¡ˮ
22 Ӱ푷xcЧ;(1)ҺwȱȚwһٱܶȞwһǧʽ͂|(zh)ЧҪ;(2)ʷ̶̣ȿЧ(3)ҺɫVУͨ^Ƃ|(zh)(4)ظ׃ϴҺMOǸƷxֱӵء(5)ٴ0.5 cm/sr(sh), Huһбʲֱ٣Ч߲Ǻܴڌ(sh)HУһ(g){(dio)xȺͳr(sh)gҪx(sh)(6)ɫVеĹ̶Һԭt϶ҺɫVxԭtcɫVһڸЧҺɫVxƂһ(xing)g(sh)ҪdzߵĹһƂ
|(zh)V
2 |(zh)Vã(zhn)_y(c)|(zh)ķ;|(zh)VΨһԴ_ʽķ;(j)ƬM(jn)лĽY(ji)(gu)
3 |(zh)VĻԭ|(zh)V늴ŌW(xu)ԭy(c)Ʒӽxɾвͬ|(zh)xȻ|(zh)ɱ(m/z)ĴСռ|(zh)V(j)|(zh)Vеķxӷ(M+)ԫ@ØƷӵ(du)|(zh)Ϣ;(j)xӷ(xӷ塢ͬλxӷƬxӷ塢(wn)xӷxӷ)(du)(qing)Ⱥ͵(sh)Ҏ(gu)tԴ_ķʽ;(j)xӷ弰|(zh)W(xu)IĔҎ(gu)ɿM(jn)жԷͽY(ji)(gu);(j)M|(zh)VķcgľP(gun)ϵM(jn)ж
4 |(zh)V^̣1M(jn)ͨ^x2xӻxңMַӱһײײʹxγx3xҲײ(qing)ҶγƬx4xӱ늉Va(chn)һٶvc|(zh)늺ɼ늉P(gun)5xM(jn)һ(g)(qing)ȞBĴň(chng)(|(zh))l(f)ƫD(zhun)
5 |(zh)VxĽMɣϵy(tng)M(jn)ϵy(tng)xԴxҡ|(zh)xәzy(c)
6 ϵy(tng)ãǜpxײpʧնȵͣ(hu)xԴğz;(hu)ʹɔ_|(zh)VD;~x-ӷ(yng)׃ѽģʹ|(zh)Vጏ(f)s;ɔ_xԴ{(dio)(ji);xӵĎǧ߉(hu)늵
7 M(jn)ϵy(tng)ĿģЧ؏(f)،Ʒ뵽xԴвҲնȵĽ͡gЪʽM(jn)ϵy(tng)——wͷc(din)ד]l(f)Һw;ֱ̽M(jn)——߷c(din)Һww;ɫVM(jn)ϵy(tng)——ЙC(j)
8 xԴxңʹԇеԭxxӰ|(zh)Vx`ȺͷֱʱI(lng)8xԴc(din)x늉70eV;һСň(chng)x;EIԴxЧʸ,ƬxӶY(ji)(gu)ϢSИ(bio)(zhn)|(zh)V;Y(ji)(gu)(jin);ƷښB(ti)xĘƷܷҪښ-|(zh)(lin)Ãx;ЩƷòx
9 W(xu)xԴc(din)xС|(zh)V唵(sh)VD(jin);(qing)(M+1)+(zhn)xӷ;my]l(f)ԇ
10 ԭZԴXeԭZͿڰϵĘƷRxmڸߘOԡ᷀(wn)ԲĘƷFABһʽ|(zh)VxԴ
11 늇FԴY(ji)(gu)(ë(x))FԭFl(f)늉c(din)ESIܛһNxʽֻa(chn)xa(chn)Ƭx;mڏ(qing)OĘƷ|(zh)ǵ;a(chn)xӎж늺;ҪҺɫV-|(zh)V(lin)ÃxҺɫV|(zh)Vx֮gĽӿbͬr(sh)xbá
12 (chng)xԴ(FI) ͈(chng)xԴ(FD)xӷ及(qing);:Ƭxӷ;mϻY(ji)(gu)b
13 |(zh)oxc(din)(zhn)xӷ(qing)ƬxͨwЕr(sh)g|(zh)VemϜy(c)|(zh)DNAƬΡǵȵ(du)|(zh)
14 |(zh)ãxԴa(chn)xӰ|(zh)ɱm/zĴС_
15 ξ۽xӵm/zcR,B, VP(gun)ͨ^׃ň(chng)Ѳͬxӷ_-һŸБ(yng)(qing)B£׃늉VʹͬxȺͨ^zy(c)(sh)F(xin)|(zh)õ|(zh)Vc(din)Y(ji)(gu)(jin)Σ;ֻз۽o۽ֱʵ͡
16 p۽(sh)F(xin)۽(ٶ)۽;(du)ڄ(dng)ܲͬxӣͨ^{(dio)(ji)늈(chng)_(d)۽Ŀc(din)ֱʸ
17 ļ(j)U|(zh)c(din)Y(ji)(gu)(jin)weСpʿmcɫV(lin)C(j)
18 wЕr(sh)g|(zh)c(din)|(zh)ʿȲň(chng)Ҳ늈(chng)ֻҪֱƯƿg
19 x|(zh)ضm/zx(ni)һ܉Ϸ(wn)D(zhun)׃늘O늉ͬm/zxw嵽_(d)zy(c)c(din)Y(ji)(gu)(jin)ڲ`ȸ
20 |(zh)Vıʾ|(zh)VһþVVɷNʾþV;Vϵĸlֱʾһ(g)xӷM(bio)|(zh)ɱm/zv(bio)xӵ(du)(qing)((du)S)һ㌢ԭʼ|(zh)VD(qing)xӷ嶨岢(du)(qing)100%xӷԌ(du)(du)ٷֵʾ܉ֱ^^쵽(g)ӵ|(zh)Vȫò;|(zh)Vñʽʾ|(zh)V(sh)(j)|(zh)VЃ(xing)|(zh)ɱȼ(du)(qing)(du)Ӌ(j)^ֱ^
21 |(zh)Vxķֱʣֱ(R)ָ|(zh)Vx܅^(q)eɂ(g)|(zh)V(du)ɂ(g)ȏ(qing)ȵ(dng)ɷgķȲ10%r(sh)tJ(rn)ɷѽ(jng)_
22 |(zh)VDҪxӷͣxӷͬλxӷƬxӷ(wn)xӷxӷ
23 (du)|(zh)Ĝy(c)xӷm/zஔ(dng)ԓ(du)|(zh)һͬλxӷxӷ|(zh)VD|(zh)ɱȵķ壬λ|(zh)VDҶ
24 _J(rn)xӷķ(1)xӷ횷ϵ(sh)Ҏ(gu)tЙC(j)ﺬż(sh)(g)ԭӻԭxӷm/zһż(sh);攵(sh)(g)ԭxӷm/zһ攵(sh)(2)xӷcxӷ|(zh)(yng)粻ܳF(xin)ȷxӷ|(zh)С413(g)|(zh)λķ(3)(dng)кS,Br, Clr(sh)M+, (M+2) +ͬλxӷı_J(rn)xӷ(4)׃|(zh)VxIJl߷xӷ(du)(qing)ûW(xu)xԴZԴ늉ɫ@^(qing)M+塣
25 ɫV-|(zh)V(lin)Ãx|(zh)V|(zh)Y(ji)(gu)ɫVxɫV-|(zh)V(lin)ãͬ(yu)c(din)GC-MS;LC-MS;CE-MSɫV|(zh)VM(jn)Ӽxϵy(tng);|(zh)VɫVęzy(c)Ҫ}ӿڼg(sh);ȥɫVд(dng)m÷mړ]l(f)ȵy⻯Oԏ(qing)(du)|(zh)᷀(wn)ԲĘƷ
26 opzy(c)xopzy(c)g(sh)Ɖԙzy(c)ڲƉĴy(c)|(zh)ԭĠB(ti)W(xu)|(zh)ǰ@ȡcy(c)Ʒ|(zh)P(gun)ă(ni)|(zh)ɷֵW(xu)(bo)õęz鷽